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A NEW METHOD OF PREPARING PHOTOGRAPHIC GELATINE EMULSION BY PRECIPITATION OF THE BROMIDE OF SILVER

- FRANZ STOLZE

I began at first with a thirtieth of the whole quantity of gelatine, and increased that quantity to a tenth without the precipitate forming with greater difficulty. The salts were dissolved in the usual quantity of water, the bromide of potassium was added to the separately-dissolved gelatine, and both solutions cooled in iced water. I soon found that even this was not necessary. I accelerated the solution of the salts by vigorous agitation, so that the temperature became so much lowered that, even after the addition of the warm gelatine, it still remained low enough to give the precipitate when mixed. The mixing took place gradually, all the usual precautionary measures being observed; such as pouring the silver solution into No. 2 in small quantities at a time, and constantly stirring, and the separation from the mother lye was complete.

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