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ANALYSIS OF OILS, OR MIXTURES OF OILS, USED FOR LUBRICATING PURPOSES.

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The authors give two different processes for the determination of animal or vegetable oils or fats and hydrocarbon or other neutral oils. They take a certain weight of the sample and boil it with twice its weight of an eight per cent, solution of caustic soda in alcohol. The soda combines with the fatty acids of the animal or vegetable oils forming soaps; bicarbonate of soda is then added to neutralize the excess of caustic soda; and, lastly, sand; and the whole is evaporated to dryness at the temperature of boiling water. The dry mixture is then transferred to a large glass tube, having a small hole in the bottom plugged with glass wool to act as a filter, and light petroleum spirit--which boils at about 150° to 180° Fahr.--is poured over it, till all the neutral or unsaponifiable oil is dissolved out. In the other process no sand is used, but the dry mixture is dissolved in water, and the soap solution which holds the neutral oils in solution is treated with ether, which dissolves out the neutral oil and then floats to the surface of the liquid.

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